FT Microreactor
"Trigram-fish-shaped microreactor" FT series are the microchannel reactors independently developed by the collaboration of FLUKO and Tianjin University, with the intellectual property rights (patent design).Based on many years of R&Dresults, application experiences and deep understanding of reaction process, the collaborated team has successfully designed and explored the "Trigram-fish-shaped reactor", expanding the performance of microchannel reactors.
"Trigram-fish-shaped microreactor" FT series have the advantages of large specific surface area, high mass and heat transfer efficiency, high safety, and small scale-up effect.Compared with traditional batchreactors, the microreactors cancontrol precisely the feeding rate, reaction temperature, reaction pressure and reaction time; and provide more reproducibility, longer stabilityand higher efficiency during the process optimization and scale-up, occupying smaller space and implementing continuously andautomatically, as well as significantly saving the production time and costs. "Trigram-fish-shaped microreactor" FT series adoptthe core techniques of microfluidics and are suitable for most chemical reaction processes, representing the new perspective of green chemical processes.
The materials of the FT series reactors can be selected as various metals, glass, silicon carbide and so on, according to the actualprocess conditions of individual customers, aiming at shortening the reaction time, reducing the material consumption andimproving the reaction conversion rate, the selectivity, the product yield and quality, reducing production costs and environmen-tal pollution. The FT series can accomplish successfully the reliable transfer and scale-up from the laboratory, the pilot to theindustrial production, covering the overall scale-levels.
Application fields of FT series microchannel reactor
Fine chemicals,pharmaceuticals, nanomaterials, petrochemicals, high-risk chemistry, biochemistry, polymerchemistry and other chemical fields.
Suitable reaction types
Fast and heavily exothermic reactions: nitration, sulfonation, rearrangement, ion polymerization, alkylation, etc. High-risk reactions: hydrogenation, halogenation, oxidation, peroxidation, phosgenation, diazo coupling reaction, reoxidation reaction, etc.
Extreme conditions: supercritical, ultra-low & high temperature, ultra-high pressure reactions, etc. New reactions: photochemical, electrochemical reactions, etc.
High-viscosity, solid-containing reaction system can choose FLUKO's " high-shear reaction equipment".
Glass reactors are suitable for chemical reactions in laboratories and industries. Such as: decomposition reaction, compound reaction, metathesis reaction, redox reaction, electrochemical reaction, hydrolysis reaction, esterification reaction, saponification reaction, polymerization reaction, etc. The system is modular in design, and the processing capacity is from 10L to 100L. It is flexible, reliable and durable. It has complete accessories such as multifunctional mixing, vacuum, distillation and condensation, and can be replaced or integrated with other components at any time.
The microchannel design of "Trigram-fish-shaped" takes into account the comprehensive optimization of mixing, mass transfer, heat transfer and pressure drop; the structure of "sudden expansion and sudden contraction" can efficiently utilize the energy dissipation in microchannel; while the structure of "Trigram fish eye" can simultaneously realize the collision, fragmentation and diversion of fluid, ensure the efficiently mixing effect and increase the mass transfer area of multiple phases, so as to achieve low pressure drop under the same mixing and mass transfer efficiency; new double-sided heat transfer technology provides the system with highly efficient heat transfer properties.
TECHNICAL PARAMETER
G10 | |
Power supply | 220V,50/60Hz |
Vessel capacity | 10L |
Glass material | High borosilicate glass GG-17 |
Frame material | SS304 |
Vessel cover material | High borosilicate glass GG-17 |
Vessel cover diameter | 265mm |
Cover ports quantity | 7 |
Mixer motor power | 120W |
Speed adjustment type | Frequency control |
Rotation speed range | 50~400rpm |
Temperature range | -60~200℃ |
Digital display | Rotation speed, medium temperature |
Type of seal | Mechanical seal |
Maximum vacuum degree | < 20mbar |
Material of mixer shaft | SS304 coated with PTFE |
Type of mixer agitator | Screw type |
Type of temperature meter | PT100 digital |
Vacuum meter | Indicator |
Discharging valve | Bottom discharge with PTFE |
Outlet | Bottom discharge |
Condenser type and heat transfer area of condensation recovery | Double layer screw shape 0.40㎡ |
Constant pressure hopper | 500mL |
Divide bottle | 250mL with valve |
Collect bottle | 5L - NS24×2 with bottom valve |
Temperature measurement port | NS24 |
Liquid medium valve/Air intake valve | NS29 |
Condensing port | NS34 |
Spare ports | F50 x2(PH/conductivity meter by customer) |
Solid feeding port | SF110 |
Liquid leakage plate | SS316 - removable plate |
Caster | Load bearing brake casters |
Vessel bottom valve O ring | FFKM |
Mixing O ring | FFKM |
Vessel cover and diverter valve O ring | coated with PTFE |
Jacket O ring | FKM |
Other position O ring-blind plate/bottom valve gasket etc | EPDM |
Thermal insulation sleeve | Available |
Overall dimensions | 900×500×1900 |
Model | Material | Designed temperature | Designed pressure | Reaction volume | Flow rate | Annual processing capacity |
FT1 | SS316L(special glass, SiC) |
-50~300℃ (special glass, SiC:-40~200℃) |
0-300bar (special glass, SiC:0-20bar) |
0.6mL | 1.0~10.0 mL/min | 0.5~5t/a |
FT2 | SS316L |
-50~300℃ (special glass, SiC:-40~200℃) |
0-300bar (special glass, SiC:0-20bar) |
3.6mL | 10.0~200.0 mL/min | 5~100t/a |
FT3 | SS316L |
-50~300℃ (special glass, SiC:-40~200℃) |
0-300bar (special glass, SiC:0-20bar) |
45mL | 200~2000 mL/min | 100~1000t/a |
FT4 | SS316L |
-50~300℃ (special glass, SiC:-40~200℃) |
0-300bar (special glass, SiC:0-20bar) |
180mL |
2000~10000 mL/min |
1000~4800t/a |
FT5 | SS316L |
-50~300℃ (special glass, SiC:-40~200℃) |
0-300bar (special glass, SiC:0-20bar) |
500mL | 5000~20000 mL/min | 5000~10000t/a |